| Table 1 | |
| Time (s) | volume (mL) |
| 30 | 11 |
| 60 | 17 |
| 90 | 33 |
| 120 | 49 |
| 150 | 65 |
| 180 | 80 |
| 210 | 94 |
| 240 | 107 |
| 270 | 117 |
| 300 | 126 |
| 330 | 134 |
| 360 | 142 |
| 390 | 149 |
| 420 | 154 |
| 450 | 160 |
| 480 | 164 |
| 510 | 168 |
| 540 | 171 |
| 570 | 173 |
| 600 | 176 |
| 630 | 178 |
| 660 | 180 |
| 690 | 181 |
| 720 | 183 |
| 750 | 184 |
| 780 | 185 |
| 810 | 186 |
| 840 | 187 |
| 870 | 188 |
| 900 | 188 |